ISO 3924:2019
ISO 3924:2019
Petroleum products - Determination of boiling range distribution - Gas chromatography methodstandard by International Organization for Standardization, 07/01/2019
standard by International Organization for Standardization, 07/01/2019
ISO 3924:2019 specifies a method for the determination of the boiling range distribution of petroleum products. The method is applicable to petroleum products and fractions with a final boiling point of 538 C or lower at atmospheric pressure as determined by this document. This document does not apply to gasoline samples or gasoline components. The method is limited to products having a boiling range greater than 55 C and having a vapour pressure sufficiently low to permit sampling at ambient temperature.
The document describes two procedures.
a) Procedure A allows a larger selection of columns and analysis conditions, such as packed and capillary columns as well as a thermal conductivity detector in addition to the flame ionization detector. Analysis times range from 14 min to 60 min.
b) Procedure B is restricted to only three capillary columns and requires no sample dilution. The analysis time is reduced to about 8 min.
Both procedures have been successfully applied to samples containing fatty acid methyl esters (FAME) up to 20 % (volume fraction).
NOTE For the purposes of this document, the terms % (mass fraction) and % (volume fraction) are used to represent the mass fraction (), the volume fraction () of a material.